HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 58288506, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Fluoro-5-nitrobenzaldehyde | HCID 2734770 | — |
| Reactant | Ethyl 2-(3-hydroxy-4-methoxyphenyl)acetate | HCID 5324706 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 58288506 | HCID 58288506 | — |
Reaction Conditions
| Temperature | 100 °C |
|---|
Reaction Steps
2-Fluoro-5-nitrobenzaldehyde (8.8 g, 52 mmol), (3-hydroxy-4-methoxy-phenyl)-acetic acid ethyl ester (10.0 g, 48 mmol), and potassium carbonate (10.0 g, 69 mmol) were combined in 1,4-dioxane (150 mL), and the reaction was stirred at 100° C. for 24 hours. The mixture was worked up to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08426449B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-9f8001a4f35e41d7a18c494b191ae11e |
| Source note | uspto-grants-2013_04 |