HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine → HCID 58288476, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | Sodium cyanoborohydride | HCID 5003444 | — |
| Reactant | HCID 58288506 | HCID 58288506 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 58288476 | HCID 58288476 | — |
Reaction Steps
[3-(2-Formyl-4-nitro-phenoxy)-4-methoxy-phenyl]-acetic acid ethyl ester (1.0 g, 2.79 mmol), ethylamine (2M in THF; 2.8 mL, 5.6 mmol), and sodium cyanoborohydride (0.26 g, 4.2 mmol) were combined in CH2Cl2 (30 mL), and the reaction was stirred at room temperature for 3 hours. After work-up, the mixture was concentrated to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08426449B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-5fb5000e6b17484f876be21bd036822f |
| Source note | uspto-grants-2013_04 |