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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1969090Generated: October 31, 2026

Triethylamine → HCID 58288509, compound

https://huagongshe.com/reaction/1969090

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethylamineHCID 8471—
Reactant4-Chlorobenzoyl chlorideHCID 8501—
ReactantHCID 58288533HCID 58288533—
SolventDichloromethaneHCID 6344—
ProductHCID 58288509HCID 58288509—

Reaction Steps

(3-{4-Amino-2-[(benzyloxycarbonyl-ethyl-amino)-methyl]-phenoxy}-4-methoxy-phenyl)-acetic acid ethyl ester (0.1 g, 0.19 mmol), 4-chlorobenzoyl chloride (0.1 g, 0.57 mmol), and triethylamine (0.5 mL, 3.6 mmol) were combined in CH2Cl2 (10 mL) and stirred at room temperature for 20 minutes. The mixture was concentrated to give the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08426449B2
Source datasetuspto-grants-2013_04
ORD IDord-e4b3ee9f34a94350afce4df654cf342d
Source noteuspto-grants-2013_04