HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 58288509, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-Chlorobenzoyl chloride | HCID 8501 | — |
| Reactant | HCID 58288533 | HCID 58288533 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 58288509 | HCID 58288509 | — |
Reaction Steps
(3-{4-Amino-2-[(benzyloxycarbonyl-ethyl-amino)-methyl]-phenoxy}-4-methoxy-phenyl)-acetic acid ethyl ester (0.1 g, 0.19 mmol), 4-chlorobenzoyl chloride (0.1 g, 0.57 mmol), and triethylamine (0.5 mL, 3.6 mmol) were combined in CH2Cl2 (10 mL) and stirred at room temperature for 20 minutes. The mixture was concentrated to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08426449B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-e4b3ee9f34a94350afce4df654cf342d |
| Source note | uspto-grants-2013_04 |