HRID1969090

反应详情

EQUATION

反应方程式

HRID 1969090 反应方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

(3-{4-Amino-2-[(benzyloxycarbonyl-ethyl-amino)-methyl]-phenoxy}-4-methoxy-phenyl)-acetic acid ethyl ester (0.1 g, 0.19 mmol), 4-chlorobenzoyl chloride (0.1 g, 0.57 mmol), and triethylamine (0.5 mL, 3.6 mmol) were combined in CH2Cl2 (10 mL) and stirred at room temperature for 20 minutes. The mixture was concentrated to give the title compound.

WORKUP

后处理

  1. concentrationThe mixture was concentrated