Hydroxylamine → HCID 77066184, compound

HRID 1969146Notes

Reaction equation

HRID 1969146 reaction equation
[CH:1]([C:3]1[CH:4]=[CH:5][C:6]([O:11][CH3:12])=[C:7]([CH:10]=1)[C:8]#[N:9])=O.C([O-])(=O)C.[Na+].[OH:18][NH2:19]>C(O)C>[OH:18][N:19]=[CH:1][C:3]1[CH:4]=[CH:5][C:6]([O:11][CH3:12])=[C:7]([CH:10]=1)[C:8]#[N:9]

Participants

5

Reactant 3

HCID 787HydroxylamineHCID 517045Sodium AcetateHCID 226207855-Formyl-2-methoxybenzonitrile

Product 1

HCID 77066184HCID 77066184, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Conditions

Temperature
80 °C

Procedure

5-Formyl-2-methoxybenzonitrile, sodium acetate and hydroxyamine were dissolved in ethanol, followed by stirring at 80° C. for 6 hours to obtain 5-[(hydroxyimino)methyl]-2-methoxybenzonitrile. APN: 175.

Sources & evidence

ORD record
ord-d9b93728fdb3489f93f322b7d012b598
Source dataset
uspto-grants-2013_04
Patent number
US08426453B2

Reaction notes

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