HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 25117629, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | HCID 25117631 | HCID 25117631 | — |
| Product | HCID 25117629 | HCID 25117629 | — |
Reaction Steps
Methyl 4-(3-carboxy-propionylamino)-2-hydroxybenzoate (1 g) from Example 2 is dissolved in 5 mL of 28% ammonium hydroxide solution. The reaction mixture is stirred at ambient conditions for 16 hours. In an ice-water bath, the solution is carefully acidified using concentrated hydrochloric acid. The precipitate is collected by filtration, washed with water and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08426466B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-a6dd87129eb940c1abad1ed13aa1bc99 |
| Source note | uspto-grants-2013_04 |