HCID 726575, compound → HCID 59588990, compound

Participants

Reaction Steps

This compound was synthesized from tert-butyl [(2E)-4-bromo-3-fluoro-2-methylbut-2-en-1-yl]carbamate and N-cyclohexyl-4-hydroxybenzamide following procedure F and was obtained as a colorless solid; 1H-NMR (400 MHz, CDCl3): δppm: 1.15-1.27 (3H, m), 1.37-1.48 (2H, m), 1.43 (9H, s), 1.62-1.67 (1H, m), 1.72-1.77 (2H, m), 1.76 (3H, d, J 4.0 Hz), 2.00-2.04 (2H, m), 3.77 (2H, d, J 5.7 Hz), 3.95 (1H, m), 4.61 (1H, br s), 4.75 (2H, d, J 21.4 Hz), 5.85 (1H, br s), 6.95 (2H, d, J 9.0 Hz), 7.72 (2H, d, J 9.0 Hz).

Provenance & Evidence