HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 86627484, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | 8-chlorosulfonyl-4-oxo-4,5-dihydro-3H-pyrrolo[2,3-c]quinoline-1-carboxylic acid | HCID 45121068 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86627484 | HCID 86627484 | 8.2% |
Reaction Steps
This compound is prepared according to synthesis 25, from 115 mg (0.30 mmol) of 8-chlorosulfonyl-4-oxo-4,5-dihydro-3H-pyrrolo[2,3-c]quinoline-1-carboxylic acid (synthesis 2) and 32 μL (0.36 mmol) of morpholine. After trituration in hot methanol, 5 mg (4%) of 8-(morpholine-4-sulfonyl)-4-oxo-4,5-dihydro-3H-pyrrolo[2,3-c]quinoline-1-ethyl carboxylate is obtained in the form of a gray solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08426437B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-234f5ae0978b45bf8d88d6eea961f2af |
| Source note | uspto-grants-2013_04 |