Methanesulfonyl chloride → HCID 86627490, compound

Participants

Reaction Steps

This compound is prepared according to synthesis 37, from 50 mg (0.18 mmol) of 8-amino-4-oxo-4,5-dihydro-3H-pyrrolo[2,3-c]quinoline-1-ethyl carboxylate (synthesis 64) and 17 μL (0.20 mmol) of methanesulfonyl chloride. After recrystallization from methanol, 29 mg (45%) of 8-methanesulfonylamino-4-oxo-4,5-dihydro-3H-pyrrolo[2,3-c]quinoline-1-ethyl carboxylate is obtained in the form of a white solid.

Provenance & Evidence