HuagongsheHuagongshe Chemistry Print Report · For research reference only
Styrene → 4-oxo-8-styryl-4,5-dihydro-3H-pyrrolo[2,3-c]quinoline 1-ethyl carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Styrene | HCID 7501 | — |
| Reactant | 8-bromo-4-oxo-4,5-dihydro-3H-pyrrolo[2,3-c]quinoline 1-ethyl carboxylate | HCID 86627517 | — |
| Product | 4-oxo-8-styryl-4,5-dihydro-3H-pyrrolo[2,3-c]quinoline 1-ethyl carboxylate | HCID 86627518 | 14% |
Reaction Steps
This compound is prepared according to synthesis 68, from 70 mg (0.21 mmol) of 8-bromo-4-oxo-4,5-dihydro-3H-pyrrolo[2,3-c]quinoline-1-ethyl carboxylate (synthesis 71) and 26 μL (0.23 mmol) of styrene. After filtration and trituration in diethyl ether, 10 mg (14%) of 4-oxo-8-styryl-4,5-dihydro-3H-pyrrolo[2,3-c]quinoline-1-ethyl carboxylate is obtained in the form of a light brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08426437B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-4e27c66683854fdc9a156380f23d1267 |
| Source note | uspto-grants-2013_04 |