HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 86627523, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Oxindole | HCID 321710 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | 5-acetyl-2,3-dihydro-1H-indol-2-one | HCID 10219643 | — |
| Product | HCID 86627523 | HCID 86627523 | — |
Reaction Steps
Synthesis of 5-acetyl-1,3-dihydro-indol-2-one is described by Peng Cho Tang (US2003/0069421 A1). This compound was prepared according to this procedure from 6.65 g (50 mmol) of 1,3-dihydro-indol-2-one, aluminium trichloride (150 mmol) and acetyl chloride (100 mmol) to give, after trituration in water and drying, 7.32 g (83%) of 5-acetyl-1,3-dihydro-indol-2-one in the form of a beige solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08426437B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-a7cf9bd9a6bb4db588a2ac7731b4f0e0 |
| Source note | uspto-grants-2013_04 |