Glyoxylic Acid → 951001-54-0

HRID 1970097Notes

Reaction equation

HRID 1970097 reaction equation
[C:1]([OH:5])(=[O:4])[CH:2]=[O:3].C([O-])(=O)C.[Mg+2:10].C([O-])(=O)C>>[C:1]([O-:5])(=[O:4])[CH:2]=[O:3].[Mg+2:10].[C:1]([O-:5])(=[O:4])[CH:2]=[O:3]

Participants

3

Reactant 2

HCID 760Glyoxylic AcidHCID 8896Magnesium Acetate

Product 1

HCID 86644253951001-54-0Yield 98%

Procedure

To 148 g (1.00 mol) of a 50% aqueous glyoxylic acid solution was added 355.97 g (0.5 mol) of a 20% aqueous magnesium acetate solution. The resulting solution was concentrated by means of an evaporator and further dried at 50° C. for 1 hour to obtain 83.47 g (0.49 mol, yield: 98.0%) of magnesium glyoxylate.

Workup

  1. concentrationThe resulting solution was concentrated by means of an evaporator
  2. customfurther dried at 50° C. for 1 hour

Sources & evidence

ORD record
ord-f77267958c4c416da72e6b37b2ba39d8
Source dataset
uspto-grants-2013_04
Patent number
US08426632B2

Reaction notes

Loading…