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HRID1970476

反应详情

EQUATION

反应方程式

HRID 1970476 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)C(F)(F)F
HCID6422

未命名化合物

结构：CC(C)(C)OC(=O)NC1CCN(C(=O)OCc2ccccc2)C1
HCID14555478

未命名化合物

PRODUCTS

生成物

1
结构：NC1CCN(C(=O)OCc2ccccc2)C1
HCID2756614

Benzyl 3-aminopyrrolidine-1-carboxylate

C12H16N2O2

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

To a solution of 3.21 g 3-tert-butoxycarbonylamino-pyrrolidine-1-carboxylic acid benzyl ester in 40 ml dichloromethane were added 13 ml TFA. After 16 h the solution was evaporated to give the crude hydrotrifluoroacetate. Yield: 3.20 g.

WORKUP

后处理

  1. customAfter 16 h the solution was evaporated
  2. customto give the crude hydrotrifluoroacetate