HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminothiazole → N-(thiazol-2-yl)-1H-imidazole-1-carbothioamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminothiazole | HCID 2155 | — |
| Reactant | 1,1'-Thiocarbonyldiimidazole | HCID 80264 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | N-(thiazol-2-yl)-1H-imidazole-1-carbothioamide | HCID 10750950 | 89.1% |
Reaction Steps
35 g (349.5 mmol) of 2-aminothiazole and 62.3 g (349.5 mmol) thiocarbonyldiimidazole were stirred in 1300 ml acetonitrile for a total of four days at room temperature. Filtration of the precipitate formed and drying yielded 65.5 g of light yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08431604B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-448018d97d204e7988ec440906e6f1ab |
| Source note | uspto-grants-2013_04 |