HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-Butylamine → HCID 58124811, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-Butylamine | HCID 6385 | — |
| Reactant | 5-(Thiophen-2-yl)pent-4-ynyl methanesulfonate | HCID 58124869 | — |
| Product | HCID 58124811 | HCID 58124811 | — |
Reaction Steps
A mixture of 210 mg of 2b and 5 ml of tert-butyl amine was stirred for 4 days. The reaction mixture was concentrated and the residue was treated with 20 ml of 1M K2CO3 and the product was extracted into ethyl acetate. The organic layer was washed once with water, dried and concentrated, to provide 250 mg of 2c as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08431564B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-8e0de67fab5d417e84bc9474c78ac7a0 |
| Source note | uspto-grants-2013_04 |