HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 20400313, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | 1-Hexanol, 6-[[(1,1-dimethylethyl)dimethylsilyl]oxy]- | HCID 11195649 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 20400313 | HCID 20400313 | — |
Reaction Steps
To a solution of 232 mg of alcohol 16b in 10 ml of ether was added 1 ml of triethyl amine, followed at 0° C. by 80 μl of mesyl chloride. The mixture was stirred at ambient temperature for 1 hr and then poured into water and extracted into ether. The organic extract was washed with water, dried and concentrated, to give 320 mg of 16c as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08431564B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-2dadfc70db544165b8a9f270026b3d41 |
| Source note | uspto-grants-2013_04 |