HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 68984339, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | HCID 57912459 | HCID 57912459 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 68984339 | HCID 68984339 | — |
Reaction Steps
To N-butyl-3-[4-(ethoxymethyl)-2,6-dimethoxyphenyl]-6-methoxy-N-(tetrahydro-2H-pyran-4-yl)pyrazolo[5,1-b][1,3]thiazole-7-amine (1.02 g) was added acetone (2 mL) warmed by hot water, then hydrobromic acid (8.84M, 240 μL) was added, and the mixture was stirred. The solvent in the mixture was partially removed by blowing nitrogen stream, and the mixture was further stirred.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08431603B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-4e48fd961bcc471880c0ab8bbf5ae968 |
| Source note | uspto-grants-2013_04 |