HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 68512792, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | Phosphoric Acid | HCID 1004 | — |
| Reactant | HCID 57912459 | HCID 57912459 | — |
| Solvent | Heptane | HCID 8900 | — |
| Product | HCID 68512792 | HCID 68512792 | — |
Reaction Steps
To N-butyl-3-[4-(ethoxymethyl)-2,6-dimethoxyphenyl]-6-methoxy-N-(tetrahydro-2H-pyran-4-yl)pyrazolo[5,1-b][1,3]thiazole-7-amine (2.99 g) were added ethanol (7 mL) warmed by hot water and phosphoric acid (14.6M, 410 μL). Heptane was added by 1 mL and the volume totaled 30 mL. The mixture was stirred for 1 hour under shading.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08431603B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-505b403b5e1d4d3f9b74d36032bf08ca |
| Source note | uspto-grants-2013_04 |