Ethanol → HCID 68514591, compound

Participants

Reaction Steps

To a mixture of N-(2-cyclopropylethyl)-3-[4-(ethoxymethyl)-2,6-dimethoxyphenyl]-6-methoxy-N-(tetrahydro-2H-pyran-4-yl)pyrazolo[5,1-b][1,3]thiazole-7-amine (757.0 mg), ethanol (10 mL) and ethyl acetate (5 mL) was added phosphoric acid (14.6M, 101 μL). The mixture was stirred at room temperature for 5 minutes and the solvent was removed by blowing nitrogen stream and dried to obtain the title compound (856.0 mg).

Provenance & Evidence