HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 68515773, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 57912452 | HCID 57912452 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 68515773 | HCID 68515773 | — |
Reaction Steps
To a mixture of N-(2-cyclopropylethyl)-3-[4-(ethoxymethyl)-2,6-dimethoxyphenyl]-6-methoxy-N-(tetrahydro-2H-pyran-4-yl)pyrazolo[5,1-b][1,3]thiazole-7-amine (59.6 mg), ethanol (2 mL) and ethyl acetate (1 mL) was added concentrated sulfuric acid (6.18 μL). The mixture was stirred at room temperature for 2 hours and the solvent was removed by blowing nitrogen stream and dried to obtain the title compound (66.3 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08431603B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-70759380342743ed80ae06d6c11d18c2 |
| Source note | uspto-grants-2013_04 |