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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1971798Generated: November 2, 2026

Ethanol → HCID 68515773, compound

https://huagongshe.com/reaction/1971798

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthanolHCID 702—
ReactantSulfuric AcidHCID 1118—
ReactantHCID 57912452HCID 57912452—
SolventEthyl AcetateHCID 8857—
ProductHCID 68515773HCID 68515773—

Reaction Steps

To a mixture of N-(2-cyclopropylethyl)-3-[4-(ethoxymethyl)-2,6-dimethoxyphenyl]-6-methoxy-N-(tetrahydro-2H-pyran-4-yl)pyrazolo[5,1-b][1,3]thiazole-7-amine (59.6 mg), ethanol (2 mL) and ethyl acetate (1 mL) was added concentrated sulfuric acid (6.18 μL). The mixture was stirred at room temperature for 2 hours and the solvent was removed by blowing nitrogen stream and dried to obtain the title compound (66.3 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08431603B2
Source datasetuspto-grants-2013_04
ORD IDord-70759380342743ed80ae06d6c11d18c2
Source noteuspto-grants-2013_04