HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonic Acid → HCID 86635065, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | HCID 57912450 | HCID 57912450 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 86635065 | HCID 86635065 | — |
Reaction Steps
To a mixture of N-(cyclobutylmethyl)-3-[4-(ethoxymethyl)-2,6-dimethoxyphenyl]-6-methoxy-N-(tetrahydro-2H-pyran-4-yl)pyrazolo[5,1-b][1,3]thiazole-7-amine (13.4 mg) and ethyl acetate (0.5 mL) was added methanesulfonic acid (1.69 μL). The mixture was stirred at room temperature for 1 hour and the solvent was removed by blowing nitrogen stream and dried to obtain the title compound (15.9 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08431603B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-1a28237fc3c64abd8ee62ad128b9d678 |
| Source note | uspto-grants-2013_04 |