HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 68512858, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 44482380 | HCID 44482380 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 68512858 | HCID 68512858 | — |
Reaction Steps
To a mixture of 3-[4-(ethoxymethyl)-2,6-dimethoxyphenyl]-6-methoxy-N-propyl-N-(tetrahydro-2H-pyran-3-yl)pyrazolo[5,1-b][1,3]thiazole-7-amine (8.1 mg) and ethanol (2 mL) was added concentrated sulfuric acid (0.88 μL). The mixture was stirred at room temperature for 2 hours and the solvent was removed by blowing nitrogen stream and dried to obtain the title compound (9.8 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08431603B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-61da6754c04649fda76c80553f638278 |
| Source note | uspto-grants-2013_04 |