HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonic Acid → HCID 86635066, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | HCID 57912434 | HCID 57912434 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 86635066 | HCID 86635066 | — |
Reaction Steps
To a mixture of N-(cyclobutylmethyl)-3-[2,6-dimethoxy-4-(methoxymethyl)phenyl]-6-methoxy-N-(tetrahydro-2H-pyran-4-yl)pyrazolo[5,1-b][1,3]thiazole-7-amine (26.2 mg) and ethyl acetate (1.0 mL) was added methanesulfonic acid (3.40 μL). The mixture was stirred at room temperature for 1 hour and the solvent was removed by blowing nitrogen stream and dried to obtain the title compound (31.2 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08431603B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-c5b92cf19e074156b600126a0c2eaf56 |
| Source note | uspto-grants-2013_04 |