HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68515566, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 57912441 | HCID 57912441 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 68515566 | HCID 68515566 | — |
Reaction Steps
To a mixture of 3-[2,6-dimethoxy-4-(methoxymethyl)phenyl]-6-methoxy-N-propyl-N-(tetrahydro-2H-pyran-4-yl)pyrazolo[5,1-b][1,3]thiazole-7-amine (6.98 mg) and ethyl acetate (0.5 mL) was added hydrochloric acid in diethyl ether (1M, 14.7 μL). The mixture was stirred at room temperature for 1.5 hours and the solvent was removed by blowing nitrogen stream and dried to obtain the title compound (7.84 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08431603B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-dd154217b7544b28b7eb33fdae6906f0 |
| Source note | uspto-grants-2013_04 |