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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1971813Generated: October 29, 2026

Phosphoric Acid → HCID 68515563, compound

https://huagongshe.com/reaction/1971813

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPhosphoric AcidHCID 1004—
ReactantHCID 57912431HCID 57912431—
SolventEthyl AcetateHCID 8857—
ProductHCID 68515563HCID 68515563—

Reaction Steps

To a mixture of 3-{4-[(cyclobutyloxy)methyl]-2,6-dimethoxyphenyl}-6-methoxy-N-propyl-N-(tetrahydro-2H-pyran-4-yl)pyrazolo[5,1-b][1,3]thiazole-7-amine (30.0 mg) and ethyl acetate (0.6 mL) was added phosphoric acid (14.6M, 4.00 μL). The mixture was stirred at room temperature for 5 minutes and the solvent was removed by blowing nitrogen stream and dried to obtain the title compound (36.1 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08431603B2
Source datasetuspto-grants-2013_04
ORD IDord-6576f56cdb7f4b6bb73b452360fc27c3
Source noteuspto-grants-2013_04