反应详情

To a solution of the product of example 30 (85 mg, 0.45 mmol) in DMF (1 mL), under a nitrogen atmosphere, was added potassium salt of phthalamide (96 mg, 0.52 mmol). The resulting mixture was stirred at room temperature for 1 h. The reaction mixture was quenched with a mixture of ice-water and filtered. The slightly pink solid was washed with water to give the titled compound as a white product (79 mg, 62% yield).

1. customThe reaction mixture was quenched with a mixture of ice-water
2. filtrationfiltered
3. washThe slightly pink solid was washed with water