HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenemethanamine, 3,4-dichloro- → HCID 58126881, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenemethanamine, 3,4-dichloro- | HCID 1608 | — |
| Reactant | HCID 58126903 | HCID 58126903 | — |
| Product | HCID 58126881 | HCID 58126881 | 76.4% |
Reaction Steps
Following the same procedure for Example 49 but using 1-[2-(3,5-dimethyl-piperidin-1-yl)-2-oxo-ethyl]-6-hydroxy-3-methylsulfanylmethyl-5-oxo-1,5-dihydro-imidazo[1,2-a]pyrimidine-7-carboxylic acid methyl ester from step 2 and 3,4-dichlorobenzylamine, the title product was obtained in 76.4% yield as a yellowish amorphous solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08431581B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-424c3081c4d84aafb04fe9e664507e1c |
| Source note | uspto-grants-2013_04 |