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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1972110Generated: November 5, 2026

Methyl Benzoate → HCID 67530967, compound

https://huagongshe.com/reaction/1972110

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl BenzoateHCID 7150—
ReactantDiisopropyl EtherHCID 7914—
Reactant10-Amino-1-decanolHCID 4465355—
ProductHCID 67530967HCID 6753096790%

Reaction Steps

In an argon atmosphere, a mixture of methyl benzoate (3.0 mmol), 10-aminodecan-1-ol (3.6 mmol), Zn4(OCOCF3)6O (1.25 mol % in terms of mole number) and diisopropyl ether (5.0 ml) was heated to reflux for 20 hours, and as a result, 10-aminodecyl benzoate was obtained at a yield of 90%. The yield of 10-benzoylaminodecyl benzoate was 7%.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08431709B2
Source datasetuspto-grants-2013_04
ORD IDord-ebc8f457759a4503866b8bdd74650890
Source noteuspto-grants-2013_04