HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Benzoate → HCID 67530967, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Benzoate | HCID 7150 | — |
| Reactant | Diisopropyl Ether | HCID 7914 | — |
| Reactant | 10-Amino-1-decanol | HCID 4465355 | — |
| Product | HCID 67530967 | HCID 67530967 | 90% |
Reaction Steps
In an argon atmosphere, a mixture of methyl benzoate (3.0 mmol), 10-aminodecan-1-ol (3.6 mmol), Zn4(OCOCF3)6O (1.25 mol % in terms of mole number) and diisopropyl ether (5.0 ml) was heated to reflux for 20 hours, and as a result, 10-aminodecyl benzoate was obtained at a yield of 90%. The yield of 10-benzoylaminodecyl benzoate was 7%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08431709B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-ebc8f457759a4503866b8bdd74650890 |
| Source note | uspto-grants-2013_04 |