HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Benzoate → HCID 67530536, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Benzoate | HCID 7150 | — |
| Reactant | HCID 18957288 | HCID 18957288 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 67530536 | HCID 67530536 | 66% |
Reaction Steps
In an argon atmosphere, a mixture of methyl benzoate (1.0 mmol), 6-aminohexan-2-ol (1.2 mmol), Zn4(OCOCF3)6O (1.25 mol % in terms of mole number) and toluene (1.7 ml) was heated to reflux for 46 hours, and as a result, 6-amino-2-hexyl benzoate was obtained at a yield of 66%. The yield of 6-benzoylamino-2-hexyl benzoate was 21%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08431709B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-d0ab2f60eed849aca2051af5d2b78116 |
| Source note | uspto-grants-2013_04 |