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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1972111Generated: October 30, 2026

Methyl Benzoate → HCID 67530536, compound

https://huagongshe.com/reaction/1972111

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl BenzoateHCID 7150—
ReactantHCID 18957288HCID 18957288—
SolventTolueneHCID 1140—
ProductHCID 67530536HCID 6753053666%

Reaction Steps

In an argon atmosphere, a mixture of methyl benzoate (1.0 mmol), 6-aminohexan-2-ol (1.2 mmol), Zn4(OCOCF3)6O (1.25 mol % in terms of mole number) and toluene (1.7 ml) was heated to reflux for 46 hours, and as a result, 6-amino-2-hexyl benzoate was obtained at a yield of 66%. The yield of 6-benzoylamino-2-hexyl benzoate was 21%.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08431709B2
Source datasetuspto-grants-2013_04
ORD IDord-d0ab2f60eed849aca2051af5d2b78116
Source noteuspto-grants-2013_04