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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1972114Generated: October 30, 2026

Methyl Benzoate → HCID 53410154, compound

https://huagongshe.com/reaction/1972114

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl BenzoateHCID 7150—
Reactant4-PiperidinemethanolHCID 420771—
SolventTolueneHCID 1140—
ProductHCID 53410154HCID 5341015488%

Reaction Steps

In an argon atmosphere, a mixture of methyl benzoate (1.0 mmol), piperidin-4-ylmethanol (1.2 mmol), Zn4(OCOCF2)6O (1.25 mol % in terms of mole number) and toluene (1.7 ml) was heated to reflux for 18 hours, and as a result, piperidin-4-ylmethyl benzoate was obtained at a yield of 88%. The yield of N-benzoylpiperidin-4-ylmethyl benzoate was 12%.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08431709B2
Source datasetuspto-grants-2013_04
ORD IDord-d0abb7771cbe4cd48dc6c2b6612f19c2
Source noteuspto-grants-2013_04