HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Benzoate → HCID 53410154, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Benzoate | HCID 7150 | — |
| Reactant | 4-Piperidinemethanol | HCID 420771 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 53410154 | HCID 53410154 | 88% |
Reaction Steps
In an argon atmosphere, a mixture of methyl benzoate (1.0 mmol), piperidin-4-ylmethanol (1.2 mmol), Zn4(OCOCF2)6O (1.25 mol % in terms of mole number) and toluene (1.7 ml) was heated to reflux for 18 hours, and as a result, piperidin-4-ylmethyl benzoate was obtained at a yield of 88%. The yield of N-benzoylpiperidin-4-ylmethyl benzoate was 12%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08431709B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-d0abb7771cbe4cd48dc6c2b6612f19c2 |
| Source note | uspto-grants-2013_04 |