HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Benzoate → HCID 178511723, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Benzoate | HCID 7150 | — |
| Reactant | HCID 178511715 | HCID 178511715 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 178511723 | HCID 178511723 | 99% |
Reaction Steps
In an argon atmosphere, a mixture of methyl benzoate (1.0 mmol), trans-4-aminocyclohexan-1-ol (1.2 mmol), Zn4(OCOCF3)6O (1.25 mol % in terms of mole number) and toluene (1.7 ml) was heated to reflux for 24 hours, and as a result, trans-4-aminocyclohexyl benzoate was obtained at a yield of 99%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08431709B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-b54c1234758b4a1d8ea4036e90674af3 |
| Source note | uspto-grants-2013_04 |