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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1972171Generated: October 31, 2026

Potassium Carbonate → HCID 86640987, compound

https://huagongshe.com/reaction/1972171

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantHCID 86640986HCID 86640986—
SolventEthanolHCID 702—
ProductHCID 86640987HCID 8664098774%

Reaction Conditions

Temperature40 °C

Reaction Steps

1-Benzoyl-3-(5-bromo-4-(2-methylpyridin-3-yloxy)pyridin-2-yl)thiourea (2.8 g, 6.3 mmol) and potassium carbonate (0.57 mL, 9.5 mmol) were diluted in ethanol (50 mL). The reaction was stirred at 40° C. for 5 hours, then concentrated and purified using silica gel column chromatography (eluting with ethyl acetate) to give the title compound (1.58 g, 74% yield) as light yellow solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08431713B2
Source datasetuspto-grants-2013_04
ORD IDord-6e113340037442cbae08c5387908b36e
Source noteuspto-grants-2013_04