HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1972171Generated: October 31, 2026
Potassium Carbonate → HCID 86640987, compound
https://huagongshe.com/reaction/1972171
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 86640986 | HCID 86640986 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86640987 | HCID 86640987 | 74% |
Reaction Steps
1-Benzoyl-3-(5-bromo-4-(2-methylpyridin-3-yloxy)pyridin-2-yl)thiourea (2.8 g, 6.3 mmol) and potassium carbonate (0.57 mL, 9.5 mmol) were diluted in ethanol (50 mL). The reaction was stirred at 40° C. for 5 hours, then concentrated and purified using silica gel column chromatography (eluting with ethyl acetate) to give the title compound (1.58 g, 74% yield) as light yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08431713B2 |
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| Source dataset | uspto-grants-2013_04 |
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| ORD ID | ord-6e113340037442cbae08c5387908b36e |
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| Source note | uspto-grants-2013_04 |
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