HCID 68741356, compound → HCID 59485688, compound

Participants

Reaction Steps

tert-butyl 4-(2-(3-(4-(4-chlorophenoxy)phenyl)-2-oxo-4-(3-(trifluoromethyl)phenyl)imidazo-lidin-1-yl)ethyl)piperazine-1-carboxylate (15 mg, 0.023 mmol) is dissolved in a mixture solvent of DCM (0.2 mL) and TFA (0.2 mL). The reaction mixture is stirred at room temperature for 15 min before removal of the solvent. The residue is purified by reparative LC/MS to provide the title compound; HPLC-MS calculated for C28H28ClF3N4O2 (M+H+) 545.2, found 545.2.

Provenance & Evidence