2-Bromopyridine → HCID 59485835, compound

HRID 1972264Notes

Reaction equation

[Cl:1][C:2]1[CH:33]=[CH:32][C:5]([O:6][C:7]2[CH:12]=[CH:11][C:10]([N:13]3[CH:17]([C:18]4[CH:23]=[CH:22][CH:21]=[C:20]([OH:24])[CH:19]=4)[CH2:16][N:15]([CH2:25][CH2:26][S:27]([CH3:30])(=[O:29])=[O:28])[C:14]3=[O:31])=[CH:9][CH:8]=2)=[CH:4][CH:3]=1.Br[C:35]1[CH:40]=[CH:39][CH:38]=[CH:37][N:36]=1>>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([O:6][C:7]2[CH:8]=[CH:9][C:10]([N:13]3[CH:17]([C:18]4[CH:23]=[CH:22][CH:21]=[C:20]([O:24][C:35]5[CH:40]=[CH:39][CH:38]=[CH:37][N:36]=5)[CH:19]=4)[CH2:16][N:15]([CH2:25][CH2:26][S:27]([CH3:30])(=[O:28])=[O:29])[C:14]3=[O:31])=[CH:11][CH:12]=2)=[CH:32][CH:33]=1

Participants

Reactant 2

HCID 79732-Bromopyridine

HCID 59485920HCID 59485920, compound

Product 1

HCID 59485835HCID 59485835, compound

Procedure

The title compound is prepared as described in Example 269 from Example 290 and 2-bromopyridine. HPLC-MS calculated for C29H26ClN3O5S (M+H+): 564.0, found 564.0.

Sources & evidence

ORD record: ord-4d56983b37104c2a9dc53cfd4b160302
Source dataset: uspto-grants-2013_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08431607B2

Reaction notes

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