HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59231991, compound → HCID 58529467, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59231991 | HCID 59231991 | — |
| Reactant | HCID 59232077 | HCID 59232077 | — |
| Product | HCID 58529467 | HCID 58529467 | — |
Reaction Steps
The title compound was prepared in the same manner described for the preparation of tert-butyl 4-(4-aminopyrrolo[2,1-f][1,2,4]triazin-7-yl)piperidine-1-carboxylate and substituting tert-butyl 4-(4-amino-2-methylpyrrolo[2,1-f][1,2,4]triazin-7-yl)-3,6-dihydropyridine-1(2H)-carboxylate for tert-butyl 4-(4-aminopyrrolo[2,1-f][1,2,4]triazin-7-yl)-3,6-dihydropyridine-1(2H)-carboxylate. 1H-NMR (CD2 Cl2): δ 6.59 (d, 1 H), 6.41 (d, 1 H), 5.53 (br s, 2 H), 4.18 (m, 2 H), 3.33 (m, 1 H), 2.89 (m, 2 H), 2.36 (s, 3 H), 2.03 (m, 2 H), 1.58 (m, 2 H), 1.45 (s, 9 H). MS: LC/MS (+esi), m/z=332 [M+H]. RT=2.39 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08431695B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-46677fb2929442038e0d801d7f6bd424 |
| Source note | uspto-grants-2013_04 |