Hydrochloric Acid → HCID 69327017, compound

Participants

Reaction Steps

To a solution of tert-butyl 4-[4-amino-5-(2-benzyl-2H-indazol-6-yl)pyrrolo[2,1-f][1,2,4]triazin-7-yl]azepane-1-carboxylate in MeOH (10 mL) was added 4M HCl in dioxane (5 mL). The mixture was stirred at rt for 5 h. The mixture was concentrated to dryness to afford 924 mg (100%) of the desired product, which contained trace impurities. LC-MS [M+H]+=438.28, RT=2.10 min.

Provenance & Evidence