HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon tetrabromide → HCID 58529675, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon tetrabromide | HCID 11205 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | HCID 58529601 | HCID 58529601 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 58529675 | HCID 58529675 | — |
Reaction Steps
To a cooled (0° C.) solution of 4-(4-amino-5-(2-benzyl-2H-indazol-6-yl)pyrrolo[2,1-f][1,2,4)triazin-7-yl]butan-1-ol (2.54 g, 6.16 mmol) and triphenylphosphine (2.42 g, 9.24 mmol) in tetrahydrofuran (30 mL) was added carbon tetrabromide (2.45 g, 7.39 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08431695B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-15bfe33a07c24d3e8a260502f292473b |
| Source note | uspto-grants-2013_04 |