HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59231971, compound → HCID 59232026, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59231971 | HCID 59231971 | — |
| Reactant | HCID 59232069 | HCID 59232069 | — |
| Product | HCID 59232026 | HCID 59232026 | — |
Reaction Steps
This compound was prepared in a manner similar to the bromination procedure described for the preparation of tert-butyl 4-(4-amino-5-bromopyrrolo[2,1-f][1,2,4]triazin-7-yl)piperidine-1-carboxylate, using 2-(4-amino-pyrrolo[2,1-f][1,2,4]triazin-7-yl)-ethanol as the starting material. 1H NMR (300 MHz, DMSO-d6) δ 7.83 (s, 1H), 6.64 (s, 1H), 4.75 (t, 1H), 3.65 (q, 2H), 2.96 (t, 2H); ES-MS m/z 257.3/259.2 [M+H]+, RT (min) 0.35.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08431695B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-78e0ff260fbf4bd19ffa1279e012b904 |
| Source note | uspto-grants-2013_04 |