N-Methylacetamide → methylvinyldi-(N-methylacetamido)silane

HRID 1973047Notes

Reaction equation

HRID 1973047 reaction equation
[Na].[CH3:2][NH:3][C:4](=[O:6])[CH3:5].[CH3:7][CH:8]=[CH:9][SiH:10](Cl)Cl>C1(C)C=CC=CC=1>[CH3:7][CH:8]=[CH:9][SiH:10]([N:3]([CH3:2])[C:4](=[O:6])[CH3:5])[N:3]([CH3:2])[C:4](=[O:6])[CH3:5]

Participants

5

Reactant 3

HCID 6582N-MethylacetamideHCID 5360545SodiumHCID 123837375Dichloro-methylvinylsilane

Product 1

HCID 57350309methylvinyldi-(N-methylacetamido)silane

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

The amidosilanes can be prepared, by the following illustration: mixing a sodium salt of N-methylacetamide with methylvinyldichlorosilane in an inert organic solvent such as toluene, filtering the by-produced sodium chloride from the toluene-product solution and thereafter removing the toluene by vacuum distillation to obtain the product, methylvinyldi-(N-methylacetamido)silane.

Workup

  1. filtrationfiltering the by-produced sodium chloride from the toluene-product solution
  2. customremoving the toluene
  3. distillationby vacuum distillation

Sources & evidence

ORD record
ord-95addf004be247f9814a4d84f79c6e3f
Source dataset
uspto-grants-1976_12
Patent number
US03996184

Reaction notes

Loading…