HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → HCID 21492561, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 21492566 | HCID 21492566 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21492561 | HCID 21492561 | — |
Reaction Steps
2-(Chlorodiphenylmethyl)-4,5,6,7-tetrahydro-1H-1,3-diazepine hydrochloride (0.003 mole) is stirred at room temperature for two days in dry methanol (25 ml) containing sodium methoxide (0.006 mole). After removal of the solvent the residue is dissolved in chloroform washed with water and dried over magnesium sulphate. Removal of the solvent gives the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03996207 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-c0b2044b9f9a4ff18f518edda9f43e80 |
| Source note | uspto-grants-1976_12 |