Sodium Methoxide → HCID 21492562, compound

HRID 1973054Notes

Reaction equation

HRID 1973054 reaction equation
Cl.Cl[C:3]([C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)([C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)[C:4]1[NH:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][N:11]=1.[CH3:24][O-:25].[Na+]>CO>[CH3:24][O:25][C:3]([C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)([C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)[C:4]1[NH:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][N:11]=1

Participants

4

Reactant 2

HCID 10942334Sodium MethoxideHCID 21492555HCID 21492555, compound

Product 1

HCID 21492562HCID 21492562, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

2-(Chlorodiphenylmethyl)-1,4,5,6,7,8-hexahydro-1,3-diazocine hydrochloride (0.001 mole) is stirred at room temperature for 2 days in a solution of dry methanol (5 ml) containing sodium methoxide (0.002 mole). After removal of solvent the residue is dissolved in chloroform and washed with water. After drying over magnesium sulphate the solvent is removed to give the title compound.

Workup

  1. customAfter removal of solvent the residue
  2. dissolutionis dissolved in chloroform
  3. washwashed with water
  4. dry with materialAfter drying over magnesium sulphate the solvent
  5. customis removed

Sources & evidence

ORD record
ord-66cd2c02169940009e04808db252986e
Source dataset
uspto-grants-1976_12
Patent number
US03996207

Reaction notes

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