HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → HCID 21492562, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 21492555 | HCID 21492555 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21492562 | HCID 21492562 | — |
Reaction Steps
2-(Chlorodiphenylmethyl)-1,4,5,6,7,8-hexahydro-1,3-diazocine hydrochloride (0.001 mole) is stirred at room temperature for 2 days in a solution of dry methanol (5 ml) containing sodium methoxide (0.002 mole). After removal of solvent the residue is dissolved in chloroform and washed with water. After drying over magnesium sulphate the solvent is removed to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03996207 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-66cd2c02169940009e04808db252986e |
| Source note | uspto-grants-1976_12 |