HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropylamine → HCID 21389351, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropylamine | HCID 6363 | — |
| Reactant | 4-Methylcyclohexanone | HCID 11525 | — |
| Product | HCID 21389351 | HCID 21389351 | — |
Reaction Steps
To a mixture of 600 g. 4-methyl cyclohexanone and 1 l. isopropylamine are added 500 g. Linde Type 3A molecular sieves. The mixture is allowed to stand overnight at room temperature, after which the sieves are removed by filtration and the excess of isopropylamine is removed in vacuo at room temperature. The residual oil is 1-methyl-N-(4-methyl cyclohexylidene)-ethylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03996227 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-8633a965d21348e0acad6067a624c848 |
| Source note | uspto-grants-1976_12 |