HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Butyn-1-ol, 4-chloro- → HCID 21492750, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Butyn-1-ol, 4-chloro- | HCID 202775 | — |
| Reactant | 1-(10,11-Dihydro-3-methoxy-8-methylthio-dibenzo[b,f]thiepin-10-yl)-piperazine | HCID 13498245 | — |
| Product | HCID 21492750 | HCID 21492750 | — |
Reaction Steps
In a manner analogous to that described in Example 5, from 1-[10,11-dihydro-3-methoxy-8-methylthio-dibenzo[b,f]thiepin-10-yl]-piperazine and 4-chloro-2-butyn-1-ol there is obtained 4-{4-[10,11-dihydro-3-methoxy-8-methylthio-dibenzo-[b,f]thiepin-10-yl]-1-piperazinyl}-2-butyn-1-ol, the dihydrochloride of which melts at 208°-210° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03996229 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-e8adcc97324c493899439934ec7ed550 |
| Source note | uspto-grants-1976_12 |