HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 178482313, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 178522730 | HCID 178522730 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178482313 | HCID 178482313 | — |
Reaction Steps
Methylamine in ethanol (20 ml., 33%) and 3-chloro-N(1H-tetrazol-5-yl)-2-quinoxalinecarboxamide (Example 5) (2 g) were stirred together at room temperature for 8 hours. The yellow solid was collected and crystallised from ethanol and heated at 120° in a vacuum. It had m.p. 292° (d) (50%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03997535 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-b2482b7b9f224be3a5e6714cb109f6d9 |
| Source note | uspto-grants-1976_12 |