Methylamine → HCID 178482313, compound

HRID 1973360Notes

Reaction equation

HRID 1973360 reaction equation
[CH3:1][NH2:2].Cl[C:4]1[C:5]([C:14]([NH:16][C:17]2[NH:21][N:20]=[N:19][N:18]=2)=[O:15])=[N:6][C:7]2[C:12]([N:13]=1)=[CH:11][CH:10]=[CH:9][CH:8]=2>C(O)C>[CH3:1][NH:2][C:4]1[C:5]([C:14]([NH:16][C:17]2[NH:21][N:20]=[N:19][N:18]=2)=[O:15])=[N:6][C:7]2[C:12]([N:13]=1)=[CH:11][CH:10]=[CH:9][CH:8]=2

Participants

4

Reactant 2

HCID 6329MethylamineHCID 178522730HCID 178522730, compound

Product 1

HCID 178482313HCID 178482313, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Methylamine in ethanol (20 ml., 33%) and 3-chloro-N(1H-tetrazol-5-yl)-2-quinoxalinecarboxamide (Example 5) (2 g) were stirred together at room temperature for 8 hours. The yellow solid was collected and crystallised from ethanol and heated at 120° in a vacuum. It had m.p. 292° (d) (50%).

Workup

  1. customThe yellow solid was collected
  2. customcrystallised from ethanol
  3. temperatureheated at 120° in a vacuum

Sources & evidence

ORD record
ord-b2482b7b9f224be3a5e6714cb109f6d9
Source dataset
uspto-grants-1976_12
Patent number
US03997535

Reaction notes

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