HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 86734256, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 22917218 | HCID 22917218 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 86734256 | HCID 86734256 | — |
Reaction Steps
3,4-Dihydro-6-methoxy-3-oxo-2-quinoxalinecarboxylic acid, ethyl ester (1.9 g), methyl iodide (2 ml) and anhydrous potassium carbonate (6 g) in 2-butanone (100 ml) were stirred and heated under reflux for 1.5 hours. The solid was filtered off and the filtrate was evaporated. The residue was crystallised from aqueous methanol, m.p. 166° (80%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03997535 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-3d611fe40f674a7791b034bd340283e1 |
| Source note | uspto-grants-1976_12 |