HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylene Glycol → HCID 21491989, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylene Glycol | HCID 174 | — |
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 21491925 | HCID 21491925 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 21491989 | HCID 21491989 | — |
Reaction Steps
Twenty parts 4-cyano-2,5-diisopropylbenzenesulfonamide is refluxed with 50 parts of potassium hydroxide and 400 parts of ethylene glycol under nitrogen for 24 hours. The cooled reaction mixture is diluted with 600 parts of water and acidified with hydrochloride acid. The precipitated product is filtered and washed with water. Drying gives 17 parts of 4-carboxy-2,5-diisopropylbenzenesulfonamide having a.m.p. of 225°-231°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03997603 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-d2a2cf982bc640b5851ec4251ecdfa79 |
| Source note | uspto-grants-1976_12 |