HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 21492138, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | HCID 21492120 | HCID 21492120 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 21492138 | HCID 21492138 | — |
Reaction Steps
To 26 parts 4-hydroxymethyl-2,5-diisopropylbenzenesulfonamide dissolved in 100 parts chloroform heated just below reflux is added hydrogen bromide in a slow stream for an hour. The organic phase is washed with aqueous sodium bicarbonate, dried over magnesium sulfate and concentrated in vacuo to give 4-bromomethyl-2,5-diisopropylbenzenesulfonamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03997603 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-b5562b82999f4030bf6f6a2164abaa3c |
| Source note | uspto-grants-1976_12 |