HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 21491941, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 21491954 | HCID 21491954 | — |
| Product | HCID 21491941 | HCID 21491941 | — |
Reaction Steps
A mixture of ammonia, 25 parts, and 2,5-diisopropyl-4-trifluoromethylbenzenesulfonyl fluoride, 7 parts, is heated for 4 hours at 100° in a Hastelloy-lined bomb. After removal of the ammonia, the crude product is stirred with water, filtered and dried. Pure product, m.p. 171°-174°, is obtained after vacuum sublimation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03997603 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-1257aa2115f54c7e804a13930feaa816 |
| Source note | uspto-grants-1976_12 |